Artyushkova, K; Leadley, S R; Shard, A G (2024) An introduction to reproducible laboratory hard x-ray photoelectron spectroscopy. Journal of Vacuum Science & Technology A, 42 (5). 052801

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Abstract

X-ray sources with a photon energy higher than 2140 eV are increasingly being used for routine X-ray photoelectron spectroscopy on lab-based instruments. This analytical approach is termed ‘HAXPES’. This article provides an overview of the current and potential future uses of lab-based HAXPES in comparison to routine XPS performed using Al Kα and Mg Kα X-ray sources. The standardization of XPS has occurred over thirty years and many of the procedures and reference works are specific to the use of Al Kα and Mg Kα X-ray sources. In this article we discuss the translation of standard XPS practices to HAXPES, indicate useful resources for HAXPES users, and highlight areas where there is a need for improved information and guidance.

Item Type:	Article
Subjects:	Nanoscience > Surface and Nanoanalysis
Divisions:	Chemical & Biological Sciences
Identification number/DOI:	10.1116/6.0003740
Last Modified:	21 Oct 2024 12:22
URI:	https://eprintspublications.npl.co.uk/id/eprint/10081